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Scope

1.1 This practice covers an experimental procedure which can be used to check one's instrumentation and technique for collecting and presenting electrochemical impedance data. If followed, this practice provides a standard material, electrolyte, and procedure for collecting electrochemical impedance data at the open circuit or corrosion potential that should reproduce data determined by others at different times and in different laboratories. This practice may not be appropriate for collecting impedance information for all materials or in all environments.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Significance and Use

The availability of a standard procedure, standard material, and standard plots should allow the investigator to check his laboratory technique. This practice should lead to electrochemical impedance curves in the literature which can be compared easily and with confidence.

Samples of a standard ferritic type 430 stainless steel (UNS 430000) used to obtain the reference plots are available for those who wish to check their equipment. Suitable resistors and capacitors can be obtained from electronics supply houses.

This test method may not be appropriate for electrochemical impedance measurements of all materials or in all environments.

Keywords

ac impedance; algorithm verification; Bode; dummy cell; equipment verification; electrochemical impedance; electrochemical impedence spectroscopy; electrochemical measurement; Nyquist; polarization resistance; steel; ICS Number Code 71.040.40 (Chemical analysis)

To find similar documents by ASTM Volume:

03.02 (Corrosion of Metals; Wear and Erosion)

To find similar documents by classification:

71.040.40 (Chemical analysis Including analysis of gases and surface chemical analysis)

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