ASTM-B975 › Standard Test Method for Measurement of Internal Stress of Metallic Coatings by Split Strip Evaluation (Deposit Stress Analyzer Method)
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Scope
1.1 This test method for determining the internal tensile or compressive stress in applied coatings is quantitative. It is applicable to metallic layers that are applied by the processes of electroplating or chemical deposition that exhibit internal tensile or compressive stress values from 500 to 145 000 psi (3.45 to 1000 MPa).
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Significance and Use
5.1 Internal stress in applied coatings exhibits potential to cause a breakdown of resistance to corrosion and erosion as a result of the formation of fractures from micro-cracking and macro-cracking within the applied coating. This phenomenon can also cause blistering, peeling, reduction of fatigue strength, and loss. The resulting stress can be tensile in nature, causing the deposit to contract, or compressive in nature, causing the deposit to expand.
5.2 To maintain quality assurance by the bent strip method, it is necessary to monitor production processes for acceptable levels of internal deposit stress in applied coatings. Note that the highest value of the internal deposit stress as obtained on a stress-versus-coating-thickness curve is usually the truest value of the internal deposit stress. Most low values are false. Initial values tend to be lower than the actual value because of the effect of stock material edge burrs and the resistance of the stock material to bending. Excessive deposit thickness causes lower-than-true values since the coating overpowers and changes the initial modulus of elasticity of the test piece, which becomes more difficult to bend as the coating continues to build upon it. This phenomenon can be corrected considerably by use of a formula that compensates for modulus of elasticity differences between the deposit and the substrate materials, but it does remain a factor. See Eq 2.
Keywords
deposit stress analyzer method; helix; internal deposit stress; metallic coatings; modulus of elasticity; spiral contractometer method; test strip ;; ICS Number Code 25.220.40 (Metallic coatings)
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02.05 (Metallic and Inorganic Coatings; Metal Powders and Metal Powder Products)
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Document Number
ASTM-B0975-22
Revision Level
2022 EDITION
Status
Current
Modification Type
New
Publication Date
Dec. 14, 2022
Document Type
Test Method
Page Count
8 pages
Committee Number
B08.10