ASTM-D7771 Standard Test Method for Determination of Benzo-α-Pyrene (BaP) Content in Carbon Black

ASTM-D7771 - 2017A R22 EDITION - SUPERSEDED
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Standard Test Method for Determination of Benzo-α-Pyrene (BaP) Content in Carbon Black

Scope

1.1 This test method covers the qualitative and quantitative determination of only benzo-α-pyrene (BaP), a specific polycyclic aromatic hydrocarbon (PAH), on carbon black. The procedure involves Soxhlet extraction with toluene and analysis by gas chromatography with mass spectrometry (GC/MS). This method is not intended to test for U.S. Food and Drug Administration (FDA) compliance of carbon blacks used for indirect food contact applications.

1.2 UnitsThe values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Significance and Use

This test procedure is used to determine the concentration of BaP extracted from carbon black by the means of a Soxhlet extraction apparatus with toluene.

Keywords

BaP; benzo-a-pyrene; carbon black; GC/MS; Soxhlet extraction; toluene extract; ICS Number Code 83.040.20 (Rubber compounding ingredients)

To find similar documents by ASTM Volume:

09.01 (Rubber, Natural and Synthetic -- General Test Methods; Carbon Black)

To find similar documents by classification:

83.040.20 (Rubber compounding ingredients Including carbon black, kaolin clay, etc.)

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Document Number

ASTM-D7771-17AR22

Revision Level

2017A R22 EDITION

Status

Superseded

Modification Type

New

Publication Date

July 14, 2022

Document Type

Test Method

Page Count

10 pages

Committee Number

D24.66