ASTM-D6845 › Standard Test Method for Silica, Precipitated, Hydrated—CTAB (Cetyltrimethylammonium Bromide) Surface Area
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Scope
1.1 This test method covers the measurement of the specific surface area of precipitated silicas exclusive of area contained in micropores too small to admit hexadecyltrimethylammonium bromide (cetyltrimethylammonium bromide, commonly referred to as CTAB) molecules. This test method is suitable for characterizing rubber-grade silicas of all types.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Significance and Use
4.1 The CTAB molecule is relatively large; so it is not adsorbed in micropores or on surface roughness. Thus, the CTAB surface area reflects only the surface of the silica that is available for interaction with rubber molecules.
Keywords
cetyltrimethylammonium bromide; CTAB; silica; surface area by CTAB method; turbidity titration;
To find similar documents by ASTM Volume:
09.01 (Rubber, Natural and Synthetic -- General Test Methods; Carbon Black)
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Document Number
ASTM-D6845-22
Revision Level
2022 EDITION
Status
Current
Modification Type
Revision
Publication Date
Nov. 29, 2022
Document Type
Test Method
Page Count
4 pages
Committee Number
D11.20