ASTM-C1267 Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium

ASTM-C1267 - 2017 R22 EDITION - CURRENT
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Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
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Scope

1.1 This test method, commonly referred to as the Modified Davies and Gray technique, covers the titration of uranium in product, fuel, and scrap materials after the material is dissolved. The test method is versatile and has been ruggedness tested. With appropriate sample preparation, this test method can give precise and unbiased uranium assays over a wide variety of material types (1, 2). Details of the titration procedure in the presence of plutonium with appropriate modifications are given in Test Method C1204.

1.2 Uranium levels titrated are usually 20 to 50 mg, but up to 200 mg uranium can be titrated using the reagent volumes stated in this test method.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety precaution statements, see Section 4.

Keywords

Chromium titration of uranium; Davies and Gray titration of uranium; Modified Davies and Gray technique; Nuclear scrap and waste materials; Titration; Uranium; Uranium analysis in product/fuel; uranium, by iron (II) reduction in phosphoric acid followed by chromium; (VI) titration in presence of vanadium, test; ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)

To find similar documents by ASTM Volume:

12.01 (Nuclear Energy (I))

To find similar documents by classification:

27.120.30 (Fissile materials and nuclear fuel technology Including raw materials Radioactive wastes, see 13.030.30)

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Document Number

ASTM-C1267-17R22

Revision Level

2017 R22 EDITION

Status

Current

Modification Type

Revision

Publication Date

July 26, 2022

Document Type

Test Method

Page Count

10 pages

Committee Number

C26.05