ASTM-C1267 › Standard Test Method for Uranium by Iron (II) Reduction in Phosphoric Acid Followed by Chromium (VI) Titration in the Presence of Vanadium
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Scope
1.1 This test method, commonly referred to as the Modified Davies and Gray technique, covers the titration of uranium in product, fuel, and scrap materials after the material is dissolved. The test method is versatile and has been ruggedness tested. With appropriate sample preparation, this test method can give precise and unbiased uranium assays over a wide variety of material types (1, 2). Details of the titration procedure in the presence of plutonium with appropriate modifications are given in Test Method C1204.
1.2 Uranium levels titrated are usually 20 to 50 mg, but up to 200 mg uranium can be titrated using the reagent volumes stated in this test method.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific safeguard and safety precaution statements, see Section 4.
Keywords
Chromium titration of uranium; Davies and Gray titration of uranium; Modified Davies and Gray technique; Nuclear scrap and waste materials; Titration; Uranium; Uranium analysis in product/fuel; uranium, by iron (II) reduction in phosphoric acid followed by chromium; (VI) titration in presence of vanadium, test; ICS Number Code 27.120.30 (Fissile materials and nuclear fuel technology)
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Document Number
ASTM-C1267-17R22
Revision Level
2017 R22 EDITION
Status
Current
Modification Type
Revision
Publication Date
July 26, 2022
Document Type
Test Method
Page Count
10 pages
Committee Number
C26.05